In-situ synchrotron diffraction analysis of deformation mechanisms in an AA5083 sheet metal processed by modified equal-channel angular pressing (bibtex)

by M. Gruber, S. Vitzthum, R. Norz, C. Illgen, W. Gan, E. Maawad, M. Hofmann, M. Böhme, P. Frint, M. F.-X. Wagner, C. Hartmann, W. Volk

Abstract:
Severe plastic deformation (SPD) is a process to significantly improve the mechanical properties of materials by grain refinement. For forming at room temperature (RT), higher strengths can thus be achieved; for increased temperatures (HT), greater elongations can be achieved. This great potential has been chiefly applied only on laboratory scale due to a lack of industrial process design. Equal-channel angular pressing (ECAP) offers the possibility to integrate these advantages in industrial processes. This paper investigates a modified ECAP process for aluminum AA5083 sheet metal. Two passes of ECAP for sheet metal and an additional heat treatment were used. To study the material deformation on a micro-scale, in-situ synchrotron measurements at DESY (Hamburg) were performed to analyze the evolution of lattice strains and dislocation densities during tensile testing. The mechanical properties of the ECAP-processed sheet material reveal an increase in yield strength and a decrease in elongation at RT. Higher strains can be measured for the processed material at elevated test temperatures. In-situ diffraction results show a changed behavior of the ECAP sheet material compared to the reference material for both temperature regimes. These changes are based on the increased defect density in the material, which leads to increased strength at RT. At HT, dynamic recrystallization occurs during tensile testing, and the prevailing deformation mechanisms reconfigure. Electron backscatter diffraction (EBSD) and micrographs are used to interpret and supplement the observations. The findings provide the basis for the in-depth understanding of the deformation behavior of the material and help to apply the ECAP process on an industrial scale.
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Reference:
Gruber, M., Vitzthum, S., Norz, R., Illgen, C., Gan, W., Maawad, E., Hofmann, M., Böhme, M., Frint, P., Wagner, M. F.-X., Hartmann, C., Volk, W.: In-situ synchrotron diffraction analysis of deformation mechanisms in an AA5083 sheet metal processed by modified equal-channel angular pressing, Materials Science and Engineering: A 903, 146646, 2024.
Bibtex Entry:
@Article{Gruber2024,
  author   = {Gruber, M. and Vitzthum, S. and Norz, R. and Illgen, C. and Gan, W. and Maawad, E. and Hofmann, M. and Böhme, M. and Frint, P. and Wagner, M. F.-X. and Hartmann, C. and Volk, W.},
  journal  = {Materials Science and Engineering: A},
  title    = {In-situ synchrotron diffraction analysis of deformation mechanisms in an AA5083 sheet metal processed by modified equal-channel angular pressing},
  year     = {2024},
  issn     = {0921-5093},
  pages    = {146646},
  volume   = {903},
  abstract = {Severe plastic deformation (SPD) is a process to significantly improve the mechanical properties of materials by grain refinement. For forming at room temperature (RT), higher strengths can thus be achieved; for increased temperatures (HT), greater elongations can be achieved. This great potential has been chiefly applied only on laboratory scale due to a lack of industrial process design. Equal-channel angular pressing (ECAP) offers the possibility to integrate these advantages in industrial processes. This paper investigates a modified ECAP process for aluminum AA5083 sheet metal. Two passes of ECAP for sheet metal and an additional heat treatment were used. To study the material deformation on a micro-scale, in-situ synchrotron measurements at DESY (Hamburg) were performed to analyze the evolution of lattice strains and dislocation densities during tensile testing. The mechanical properties of the ECAP-processed sheet material reveal an increase in yield strength and a decrease in elongation at RT. Higher strains can be measured for the processed material at elevated test temperatures. In-situ diffraction results show a changed behavior of the ECAP sheet material compared to the reference material for both temperature regimes. These changes are based on the increased defect density in the material, which leads to increased strength at RT. At HT, dynamic recrystallization occurs during tensile testing, and the prevailing deformation mechanisms reconfigure. Electron backscatter diffraction (EBSD) and micrographs are used to interpret and supplement the observations. The findings provide the basis for the in-depth understanding of the deformation behavior of the material and help to apply the ECAP process on an industrial scale.},
  doi      = {https://doi.org/10.1016/j.msea.2024.146646},
  keywords = {Equal-channel angular pressing (ECAP), In-situ synchrotron diffraction, Dislocation density, Lattice strain, Aluminum AA5083 sheet metal},
  url      = {https://www.sciencedirect.com/science/article/pii/S092150932400577X},
}
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